HRID2352042

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID464

Hippuric acid

C9H9NO3

HCID24819

Phosphorus pentachloride

Cl5P

PRODUCTS

生成物

HCID11356064

Acetyl chloride, (benzoylamino)-

C9H8ClNO2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6367

Acetyl chloride

C2H3ClO

PROCEDURE

实验过程

The title compound was prepared by the chlorination of hippuric acid using phosphorus pentachloride in acetyl chloride according to a literature procedure, mp 124°-126° C. dec (McInally, I. et al J. Polymer Sci. Polymer Chem. Ed. (1977), 15, 2511, mp 125° C. dec.).