Thionyl Chloride → HCID 54264694, compound

HRID 2352137Notes

Reaction equation

HRID 2352137 reaction equation
[CH2:1]([O:9][C:10]1[CH:11]=[C:12]([C:22]([OH:24])=O)[C:13]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].O=S(Cl)[Cl:27]>>[CH2:1]([O:9][C:10]1[CH:11]=[C:12]([C:22]([Cl:27])=[O:24])[C:13]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 23162226HCID 23162226, compound

Product 1

HCID 54264694HCID 54264694, compound

Procedure

20 ml of SOCl2 was added to 4.0 g (1.23×10-2 mol) of 4-octyloxybiphenylcarboxylic acid, and the mixture was refluxed under heating for 5 hours to obtain 4-octyloxybiphenylcarboxylic acid chloride.

Workup

  1. temperaturethe mixture was refluxed
  2. temperatureunder heating for 5 hours

Sources & evidence

ORD record
ord-ff86c35f51cd45f3867f1fff5dbc5c3f
Source dataset
uspto-grants-1989_10
Patent number
US04876027

Reaction notes

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