Sodium Hydroxide → HCID 66670047, compound

HRID 2352149Notes

Reaction equation

HRID 2352149 reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9](OC=C)(=[O:11])[CH3:10].[OH-].[Na+]>O1CCOCC1.O.CO>[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH:9]([OH:11])=[CH2:10]

Participants

6

Reactant 2

HCID 14798Sodium HydroxideHCID 21889376HCID 21889376, compound

Product 1

HCID 66670047HCID 66670047, compound

Reagents, catalysts & solvents 3

HCID 887MethanolSolventHCID 962WaterSolventHCID 312751,4-DioxaneSolvent

Procedure

12 g. of styrene-vinyl acetate (prepared by General Preparation proceudure described above) were dissolved in 150 ml of dioxane in a reaction flask equipped as described above. To this was added 1.05 g of sodium hydroxide in 15 ml of water. The reaction was heated to reflux overnight. The resulting styrene-vinyl alcohol copolymer was obtained by precipitation in methanol, washed successively with water and excess methanol then dried overnight in a vacuum oven. The product was identified by spectroscopic analyses.

Workup

  1. customequipped
  2. temperatureThe reaction was heated
  3. temperatureto reflux overnight

Sources & evidence

ORD record
ord-d36d3b653d2d457eb4c1364473870b03
Source dataset
uspto-grants-1989_10
Patent number
US04876149

Reaction notes

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