HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Edukt | Furylacrylic acid | HCID 10876 | — |
| Edukt | CID 11268547 | HCID 11268547 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 12, but using 500 mg of radicicol, 568 mg of 2-furanacrylic acid, 15 ml of dry tetrahydrofuran, 707 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 746 mg of the title compound were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05597846 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-e49686f2024a42e78a6b8cd48cd94c25 |
| Quellennotiz | uspto-grants-1997_01 |