HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54164905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 2-Acetyl-5-methylthiophene | HCID 83655 | — |
| Product | HCID 54164905 | HCID 54164905 | — |
Reaction Steps
A mixture of 56.08 g of 2-acetyl-5-methylthiophene and 250 ml of N,N-dimethylformamide dimethylacetal was heated on a steam bath under an air condenser for 16 hours. The mixture was cooled in an ice bath and filtered giving 66.82 g of the desired compound, mp 118°-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876252 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-b098224720a648a995ff0b16220b1cec |
| Source note | uspto-grants-1989_10 |