HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopropanol → 4-Methyl-2-undecyl-2-oxazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopropanol | HCID 5126 | — |
| Reactant | Dodecanenitrile | HCID 17092 | — |
| Catalyst | Cadmium acetate, dihydrate | HCID 6537495 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 4-Methyl-2-undecyl-2-oxazoline | HCID 14651791 | 92% |
Reaction Steps
10.9 g (60 mmoles) of undecyl cyanide was treated with 5 g (66.6 mmoles) of DL-2-amino-1-propanol in presence of 400 mg (1.5 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 13.2 g (92%) of product was obtained on distillation at 115°-117° C./1-1.5 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876249 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-f8344ab66c5243c88cc958d57ef3bbc9 |
| Source note | uspto-grants-1989_10 |