HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lauric Acid → 4-Ethyl-2-undecyl-2-oxazoline-4-methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lauric Acid | HCID 3893 | — |
| Reactant | 2-Amino-2-ethyl-1,3-propanediol | HCID 8282 | — |
| Product | 4-Ethyl-2-undecyl-2-oxazoline-4-methanol | HCID 91186 | 90.1% |
Reaction Steps
26 g (130 mmoles) of dodecanoic acid and 31 g (260 mmoles) of 2-amino-2-ethyl-1,3-propanediol were condensed together by heating at 185°-190° C. for 30 hours. Work up and distillation of the residue at 160°-162° C./1 mm Hg gave 33.19 g (90%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876249 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-466d60dedc604236b5a36de9f323f12c |
| Source note | uspto-grants-1989_10 |