HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → 2-(2-Dodecyl)-2-imidazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2-Methyldodecanonitrile | HCID 103424 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | 2-(2-Dodecyl)-2-imidazoline | HCID 14651799 | 65% |
Reaction Steps
19.53 g (100 mmoles) of 2-cyanododecane, 8.5ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 15.5 g (65%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876249 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-88eb195044d540eeb46b2c20959d9d81 |
| Source note | uspto-grants-1989_10 |