Ethylenediamine → HCID 14651800, compound

HRID 2352210Notes

Reaction equation

HRID 2352210 reaction equation
[C:1]([C:3]([CH3:13])([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:4])#[N:2].[CH2:14](N)[CH2:15][NH2:16]>C(=S)=S>[CH3:4][C:3]([C:1]1[NH:2][CH2:14][CH2:15][N:16]=1)([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:13]

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 198440062,2-Dimethyldecanenitrile

Product 1

HCID 14651800HCID 14651800, compoundYield 62%

Reagents, catalysts & solvents 1

HCID 6348Carbon DisulfideSolvent

Procedure

18.32 g (100 mmoles) of 2-cyano-2-methyldecane, 8.5 ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 13.91 g (62%) of the product.

Workup

  1. distillationDistillation of the residue

Sources & evidence

ORD record
ord-bdba5c0bbe55404592e9833eca563d7c
Source dataset
uspto-grants-1989_10
Patent number
US04876249

Reaction notes

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