HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → 2-Dimethylaminopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 10889696 | HCID 10889696 | — |
| Reactant | CID 11268547 | HCID 11268547 | — |
| Reactant | HCID 19032996 | HCID 19032996 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, but using 365 mg of radicicol, 11-carbamoylundecanoyl chloride prepared from 900 mg of 11-carbamoylundecanoic acid, 8 ml of dry methylene chloride, 0.97 ml of pyridine and a catalytic amount of dimethylaminopyridine, 273 mg of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597846 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-214a4d0afb25438992dd66578caaa063 |
| Source note | uspto-grants-1997_01 |