HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → N,N-ditetradecylhydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Methyl 3-(Ditetradecylamino)propionate | HCID 19844206 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N-ditetradecylhydroxylamine | HCID 9910313 | 44% |
Reaction Steps
Using the general procedure of Example 2, 57.5 grams (0.116 mol) of the product of Example 7 in 450 ml of isopropanol is oxidized using 5.6 ml (0.15 mol) of 70% aqueous hydrogen peroxide solution to give 21.5 grams (44% yield) of the above-named product as a white solid melting at 94°-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876300 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-fb16ce27e1de489e82967b3e791b1962 |
| Source note | uspto-grants-1989_10 |