Benzaldehyde → HCID 54158128, compound

Participants

Reaction Steps

37.6 g of 6-nitro-2-styrylquinoline-6-nitroquinaldine, 21.2 g of benzaldehyde and 20.4 g of acetic anhydride were mixed and heated for 5 hours under reflux. After the reaction mixture was allowed to cool, 100 ml of ethyl acetate were added thereto and the deposited crystals were filtered. 41.6 g (75% of the theoretical yield) of the 6-nitro-2-styrylquinoline crystals were produced.

Provenance & Evidence