HCID 19843091, compound → HCID 13069055, compound

HRID 2352500Notes

Reaction equation

HRID 2352500 reaction equation
C(O)(=O)C(O)=O.C(N(CC)C[C:11]#[C:12][CH2:13][C:14]1([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[S:19][CH2:18][CH2:17][CH2:16][S:15]1)C.C(O)(=O)C(O)=O.COC1C=C(CCC(NC)C#CCC2(C3C=CC=CC=3)SCCCS2)C=CC=1OC>>[CH2:13]([C:14]1([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[S:19][CH2:18][CH2:17][CH2:16][S:15]1)[C:12]#[CH:11]

Participants

3

Reactant 2

HCID 19843091HCID 19843091, compoundHCID 86743485HCID 86743485, compound

Product 1

HCID 13069055HCID 13069055, compound

Procedure

Also prepared by this general method were: 2-(4-diethylaminobut-2-ynyl)-2-phenyl-1,3-dithiane oxalate, mp 144°-146° C., and 2-[4-[2-(3,4-dimethoxyphenyl)ethyl]methylaminobut-2-ynyl]-2-phenyl-1,3-dithiane oxalate, mp 144°-146° C.

Workup

  1. customAlso prepared by this general method

Sources & evidence

ORD record
ord-16d29c192d0543bc9b0bb4cc96fb978f
Source dataset
uspto-grants-1989_10
Patent number
US04877779

Reaction notes

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