HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 13469244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 4-Chloro-2-(1,1-dimethylethyl)-5-mercapto-3(2H)-pyridazinone | HCID 13469242 | — |
| Reactant | 1-tert-Butyl-4-(1-chloroethyl)benzene | HCID 14461041 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13469244 | HCID 13469244 | 72.7% |
Reaction Steps
By conducting a procedure similar to that in Synthesis Example 3 except using 1.5 g of 2-tert.-butyl-4-chloro-5-mercapto-3(2H)-pyridazinone, 10 ml of N,N-dimethylformamide, 1.0 g of anhydrous sodium carbonte and 1.4 g of 4-tert.-butyl-α-methylbenzyl chloride, there were obtained white needle-like crystals having the following physical properties (yield: 72.7%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877787 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-4720bdde5b614a15bcff44a9414aeabc |
| Source note | uspto-grants-1989_10 |