Sodium Hydroxide → HCID 23678976, compound

HRID 2352536Notes

Reaction equation

HRID 2352536 reaction equation
[NH2:1][C:2]1[CH:6]=[C:5]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[S:4][C:3]=1[C:13]([O:15]C)=[O:14].[OH-].[Na+:18]>>[NH2:1][C:2]1[CH:6]=[C:5]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[S:4][C:3]=1[C:13]([O-:15])=[O:14].[Na+:18]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 700562Methyl 3-amino-5-phenylthiophene-2-carboxylate

Product 1

HCID 23678976HCID 23678976, compound

Procedure

A mixture of methyl 3-amino-5-phenylthiophene-2-carboxylate (9.6 g) and 0.9M aqueous sodium hydroxide solution (50 ml) was stirred and boiled under reflux for 4 hours to give a solution of sodium 3-amino-5-phenylthiophene-2-carboxylate.

Workup

  1. temperatureunder reflux for 4 hours

Sources & evidence

ORD record
ord-6c69f66a52b44e82b377be22556d063a
Source dataset
uspto-grants-1989_10
Patent number
US04877793

Reaction notes

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