2-Chloropyrimidine → HCID 53728908, compound

HRID 2352562Notes

Reaction equation

[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[C:16]([C:17]=2[C:18]=1[CH2:19][O:20][CH3:21])=[CH:15][C:14]([OH:22])=[CH:13][CH:12]=3)=[O:5])[CH3:2].Cl[C:24]1[N:29]=[CH:28][CH:27]=[CH:26][N:25]=1>>[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[C:16]([C:17]=2[C:18]=1[CH2:19][O:20][CH3:21])=[CH:15][C:14]([O:22][C:24]1[N:29]=[CH:28][CH:27]=[CH:26][N:25]=1)=[CH:13][CH:12]=3)=[O:5])[CH3:2]

Participants

Reactant 2

HCID 744042-Chloropyrimidine

HCID 13392775HCID 13392775, compound

Product 1

HCID 53728908HCID 53728908, compound

Procedure

Analogously to Example 8 from 6-hydroxy-4-methoxymethyl-β-carboline-3-carboxylic acid ethyl ester and 2-chloropyrimidine, mp 128°-129° C.

Sources & evidence

ORD record: ord-65d7b3bf4b6244d3a362dc3114c540b5
Source dataset: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04877792

Reaction notes

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