HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Octyl thiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Octyl thiocyanate | HCID 29864 | — |
Reaction Steps
To a mixture of potassium thiocyanate (5.07 g, 51.7 mmol) in 30 ml of dimethylformamide (DMF) is added 1-bromooctane (5.0 g, 4.5 ml, 25.8 mmol). The mixture is stirred at 45° for 1.5 hours. It is then cooled to 0° and water and ether are added. The ether layer is washed with water and brine and stripped to give octylthiocyanate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877899 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-cefe0af436274098980354982a5520a9 |
| Source note | uspto-grants-1989_10 |