Water → HCID 11517239, compound

Participants

Reaction Steps

To a solution of 1-[2-(4-hydroxyphenyl)ethyl]-7-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyloxy)-1H-indole (50 mg) in methanol (1 mL) were added water (0.1 mL) and lithium hydroxide monohydrate (11 mg), and the mixture was stirred at room temperature overnight. The reaction mixture was purified by column chromatography on silica gel (eluent: methylene chloride/methanol=8/1-5/1) to give the title compound (20 mg).

Provenance & Evidence