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HRID2353074

反应详情

EQUATION

反应方程式

HRID 2353074 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)CC12CCC(c3ccc(C(=O)C(C)(C)Br)cc3)(CC1)CC2
HCID25258107

未命名化合物

结构：COC(=O)CC12CC3CC(C1)CC(c1ccccc1)(C3)C2
HCID53665692

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)CC12CC3CC(C1)CC(c1ccc(C(=O)C(C)(C)Br)cc1)(C3)C2
HCID59379786

未命名化合物

收率 35%

PROCEDURE

实验过程

Prepared according to the procedure described for Intermediate 9 using methyl (3-phenyl-1-adamantyl)acetate, the title compound being isolated in 35% yield: 1H NMR (CDCl3) δ 1.66 (d, 4H), 1.71 (s, 2H), 1.77 (s, 2H), 1.87 (s, 4H), 2.04 (s, 6H), 2.18 (s, 2H), 2.20-2.22 (m, 2H), 3.65 (s, 3H), 7.41 (d, 2H), 8.12 (d, 2H); GC-MS CI m/e MH+ 433.

WORKUP

后处理

  1. customPrepared