HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methylaminobenzoate → 4-(N-Methyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methylaminobenzoate | HCID 140375 | — |
| Reactant | 2-(5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)acetic acid | HCID 18177932 | — |
| Product | 4-(N-Methyl-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetamido)benzoic acid | HCID 23170852 | 55.3% |
Reaction Steps
In a manner similar to Example 4(c), by reaction of 2.46 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylacetic acid with 1.65 g ( 10 mmol) of methyl 4-methylaminobenzoate, 2.1 g (54%) of the expected product are obtained in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597839 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-9803325db62c4c6bbdbf5187f8e6799b |
| Source note | uspto-grants-1997_01 |