HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Hydroxymethyl)benzaldehyde → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Hydroxymethyl)benzaldehyde | HCID 556330 | — |
| Reactant | 3-Tert-butyl-4-methoxybenzoyl chloride | HCID 13633555 | — |
| Product | 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde | HCID 21474525 | — |
Reaction Steps
In a manner similar to Example 1(d), by reaction of 7.6 g (34 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 4.6 g (34 mmol) of 4-hydroxymethylbenzaldehyde, 5.6 g (51%) of the expected aldehyde, melting point 75°-6° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597839 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-5ce0e2926ba14ea4898c90b5c3f8ee8e |
| Source note | uspto-grants-1997_01 |