HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2353284Generated: October 31, 2026
Nitric Acid → 5-Chloro-4-nitro-2,1,3-benzoselenadiazole
https://huagongshe.com/reaction/2353284
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 5-Chloro-2,1,3-benzoselenadiazole | HCID 413575 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 5-Chloro-4-nitro-2,1,3-benzoselenadiazole | HCID 4366221 | — |
Reaction Steps
A solution of 5-chloro-2,1,3-benzoselenadiazole from Step A (800 mg, 1.80 mmol) in conc. H2SO4 (12 mL) was cooled to 0° C. and 90% HNO3 (0.8 mL) was added. After 30 min the reaction was cooled to 0° C. and diluted with H2O (10 mL). The solid was filtered off and washed with cold H2O to yield the title compound. MS: m/z=263 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07750010B2 |
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| Source dataset | uspto-grants-2010_07 |
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| ORD ID | ord-597ff823433b4667a73b3ad4cbceabb8 |
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| Source note | uspto-grants-2010_07 |
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