HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 57424363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 76529972 | HCID 76529972 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 57424363 | HCID 57424363 | — |
Reaction Steps
Benzyl [8-(2,4,5-trifluorophenyl)-1,4-dioxaspiro[4.5]dec-7-yl]carbamate (528 mg) was resolved by HPLC using a chiral AD column (13% isopropanol in heptane) to give benzyl [(7S,8R)-8-(2,4,5-trifluorophenyl)-1,4-dioxaspiro[4.5]dec-7-yl]carbamate as the slower eluting enantiomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750034B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-76d66dc2a5bb47429319d75f614bd290 |
| Source note | uspto-grants-2010_07 |