HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5-(benzyloxy)pentyl Methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 5-(Benzyloxy)pentan-1-ol | HCID 221194 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-(benzyloxy)pentyl Methanesulfonate | HCID 44627117 | — |
Reaction Steps
The 5-benzyloxypentanol (Aldrich, 0.32 g, 1.7 mmol), triethylamine (0.67 mL, 5.0 mmol), and methanesulfonyl chloride (0.19 mL, 2.5 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750039B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-e0d02ec9225c4dd0840a43d26c76bf33 |
| Source note | uspto-grants-2010_07 |