HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexanol → HCID 11590653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexanol | HCID 77970 | — |
| Reactant | 4-(Aminomethyl)-3-methoxyphenol | HCID 53404334 | — |
| Reactant | (1aS,5aR)-1,1,2-trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid | HCID 57892448 | — |
| Product | HCID 11590653 | HCID 11590653 | — |
Reaction Steps
(1aS,5aR)-1,1,2-Trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid 4-(6-hydroxy-hexyloxy)-2-methoxy-benzylamide is prepared starting from 4-aminomethyl-3-methoxy-phenol, 6-bromohexanol and (1aS,5aR)-1,1,2-trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid in analogy to the procedures given in Example 18. LC-MS: tR=1.08 min, [M+1]+=458.25.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750040B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-be30ad64743f4d9d83ec472777220f81 |
| Source note | uspto-grants-2010_07 |