HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 16042342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 1-(3-Bromopropyl)-4-nitrobenzene | HCID 10444482 | — |
| Product | HCID 16042342 | HCID 16042342 | 50.4% |
Reaction Steps
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 3-(4-nitrophenyl)propyl bromide (950 mg, 3.92 mmole), 520 mg (50% yield) of 5-[3-(4-nitrophenyl)-n-propyl]aminosalicylic acid was obtained as a pale yellow solid.: mp 229-231° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750045B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-60f461e6a0cb4bc48c5401b3695e7040 |
| Source note | uspto-grants-2010_07 |