HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178420353, compound → HCID 178511580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178420353 | HCID 178420353 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178511580 | HCID 178511580 | — |
Reaction Steps
7.2 g (16.4 mmol) of trans-dibenzyl-4-morpholino-cyclohexylamine were dissolved in 100 mL of MeOH and hydrogenated on 1.4 g of Pd/C (10%) at 30-50° C. The solvent was eliminated in vacuo and the residue was crystallised from ethanol and conc. HCl. Yield: 3.9 g (93%); m.p. 312° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750152B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-4b1d7e4fd90640f3a8a70558c1c99d08 |
| Source note | uspto-grants-2010_07 |