HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Isopropyl Acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Propane | HCID 6334 | — |
| Reactant | Propylene | HCID 8252 | — |
| Product | Isopropyl Acetate | HCID 7915 | — |
| Product | Propylene | HCID 8252 | — |
Reaction Steps
In a continuous autoclave with a reaction volume of 200 ml, at 110° C. and 40 bar, 16.9 g of propylene, 34.4 g of propane and 116.7 g of acetic acid per hour are reacted in the presence of 15.7 g of “Amberlyst 35 wet” as a catalyst. The effluent stream is decompressed, and the liquid and gaseous phase are analyzed separately by GC. At a propylene conversion of 90%, isopropyl acetate is obtained with a selectivity of over 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750194B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-b654f3cf71aa4be38d25a64d864fd9f3 |
| Source note | uspto-grants-2010_07 |