Boron tribromide → HCID 58775967, compound

HRID 2354264Notes

Reaction equation

HRID 2354264 reaction equation
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](O)([CH2:12][CH3:13])[CH2:10][CH3:11])=[CH:5][CH:4]=1.B(Br)(Br)Br>>[OH:2][C:3]1[CH:8]=[CH:7][C:6](/[C:9](=[CH:10]/[CH3:11])/[CH2:12][CH3:13])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 25134Boron tribromideHCID 12610665HCID 12610665, compound

Product 1

HCID 58775967HCID 58775967, compoundYield 86.3%

Procedure

Using a procedure analogous to Example 36C, 3-(4-methoxyphenyl)-3-pentanol (0.4 g, 2 mmol) and 1M boron tribromide (4 ml, 4 mmol) give the title compound (0.28 g, 86%).

Sources & evidence

ORD record
ord-926f2996c2a545669006ed1c1440a3c8
Source dataset
uspto-grants-2010_07
Patent number
US07750184B2

Reaction notes

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