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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2354299Generated: October 31, 2026

HCID 57616302, compound → HCID 57616356, compound

https://huagongshe.com/reaction/2354299

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57616302HCID 57616302—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
SolventEthyl AcetateHCID 8857—
ProductHCID 57616356HCID 5761635663.9%

Reaction Steps

1-{4-[2-(Benzyloxy)ethoxy]benzyl}-3-(β-D-glucopyranosyl)-5-methyl-1H-indole (32 mg) was dissolved in a mixed solvent of methanol (1 mL) and ethyl acetate (2 mL). To the solution was added 10% palladium-carbon powder (10 mg), and the mixture was stirred at room temperature under a hydrogen atmosphere for 1 hour. The insoluble material was removed by filtration, and the solvent was removed under reduced pressure to give the title compound (17 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07750145B2
Source datasetuspto-grants-2010_07
ORD IDord-e271fe3199fd4f029ae7b447a5af5c92
Source noteuspto-grants-2010_07