HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57616302, compound → HCID 57616356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57616302 | HCID 57616302 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57616356 | HCID 57616356 | 63.9% |
Reaction Steps
1-{4-[2-(Benzyloxy)ethoxy]benzyl}-3-(β-D-glucopyranosyl)-5-methyl-1H-indole (32 mg) was dissolved in a mixed solvent of methanol (1 mL) and ethyl acetate (2 mL). To the solution was added 10% palladium-carbon powder (10 mg), and the mixture was stirred at room temperature under a hydrogen atmosphere for 1 hour. The insoluble material was removed by filtration, and the solvent was removed under reduced pressure to give the title compound (17 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750145B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-e271fe3199fd4f029ae7b447a5af5c92 |
| Source note | uspto-grants-2010_07 |