Sodium borohydride → HCID 59381640, compound

Participants

Reaction Steps

To compound 3d (200 mg, 0.66 mmol) in 5 ml of THF and 15 ml of EtOH, NaBH4 (33 mg, 0.86 mmol) was added and the reaction mixture was stirred for 15 minutes. The reaction was quenched with water and extracted with CH2Cl2. The organic layer was washed with brine and dried with NaaSO2. After filtration the solvent was evaporated. The product was purified by flash chromatography using CH2Cl2/EtOAc 1:1 as an eluent.

Provenance & Evidence