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HRID 2354766作成日：2026年10月25日

1-[2-(Trifluoromethyl)benzoyl]piperazine → HCID 16035661、化合物

https://huagongshe.com/reaction/2354766

反応式

関与物質

役割名称HCID仕込み量
反応物1-[2-(Trifluoromethyl)benzoyl]piperazineHCID 16733784—
反応物6-Chloro-N-[2-(4-methoxyphenyl)ethyl]-3-pyridazinecarboxamideHCID 60859189—
生成物HCID 16035661HCID 16035661—

反応手順

Following the procedure of Example 15, making variations only as required to use 6-chloropyridazine-3-carboxylic acid [2-(4-metoxyphenyl)ethyl]amide in place of 6-chloropyridazine-3-carboxylic acid (2-cyclopropyl-2-hydroxyethyl)amide to react with piperazin-1-yl-(2-trifluoromethylphenyl)methanone, the title compound was obtained as a white solid (12% yield). 1H NMR (400 MHz, CDCl3) δ 8.04, 7.93, 7.74, 7.63, 7.56, 7.36, 7.12, 6.92, 6.81, 4.08-3.46, 3.33, 2.87.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07754711B2
出典データセットuspto-grants-2010_07
ORD IDord-034a2ed27eab4b808cafef202f581903
出典メモuspto-grants-2010_07