(4-Isopropylphenyl)hydrazine → 12-(4-Chloro-benzenesulfonyl)-5-(4-isopropyl-phenyl)-4,5,12-triaza-tricyclo[6.3.1.02,6]dodeca-2(6),3-diene

HRID 2354908Notes

Reaction equation

HRID 2354908 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][NH2:11])=[CH:6][CH:5]=1)([CH3:3])[CH3:2].[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([S:19]([N:22]2[CH:27]3[CH2:28][CH2:29][CH2:30][CH:23]2[C:24](=[CH:32]O)[C:25](=O)[CH2:26]3)(=[O:21])=[O:20])=[CH:15][CH:14]=1>>[Cl:12][C:13]1[CH:14]=[CH:15][C:16]([S:19]([N:22]2[CH:27]3[CH2:28][CH2:29][CH2:30][CH:23]2[C:24]2[CH:32]=[N:11][N:10]([C:7]4[CH:8]=[CH:9][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][CH:6]=4)[C:25]=2[CH2:26]3)(=[O:21])=[O:20])=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 2733249(4-Isopropylphenyl)hydrazineHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 6684222612-(4-Chloro-benzenesulfonyl)-5-(4-isopropyl-phenyl)-4,5,12-triaza-tricyclo[6.3.1.02,6]dodeca-2(6),3-diene

Procedure

Prepared as described in Example 5 using 4-isopropylphenylhydrazine and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-5fb66793835a4f45b3d2444241c1cea1
Source dataset
uspto-grants-2010_07
Patent number
US07754712B2

Reaction notes

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