tert-Butylhydrazine → HCID 16045164, compound

HRID 2354909Notes

Reaction equation

HRID 2354909 reaction equation
[C:1]([NH:5][NH2:6])([CH3:4])([CH3:3])[CH3:2].[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([S:14]([N:17]2[CH:22]3[CH2:23][CH2:24][CH2:25][CH:18]2[C:19](=[CH:27]O)[C:20](=O)[CH2:21]3)(=[O:16])=[O:15])=[CH:10][CH:9]=1>>[C:1]([N:5]1[C:20]2[CH2:21][CH:22]3[N:17]([S:14]([C:11]4[CH:12]=[CH:13][C:8]([Cl:7])=[CH:9][CH:10]=4)(=[O:16])=[O:15])[CH:18]([CH2:25][CH2:24][CH2:23]3)[C:19]=2[CH:27]=[N:6]1)([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 81890tert-ButylhydrazineHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 16045164HCID 16045164, compound

Procedure

Prepared as described in Example 5 using tert-butyl hydrazine and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-d6762aca85d147a9a85361fb3068f264
Source dataset
uspto-grants-2010_07
Patent number
US07754712B2

Reaction notes

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