Methylhydrazine → HCID 16045163, compound
Reaction equation
[CH3:1][NH:2][NH2:3].[Cl:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([N:14]2[CH:19]3[CH2:20][CH2:21][CH2:22][CH:15]2[C:16](=[CH:24]O)[C:17](=O)[CH2:18]3)(=[O:13])=[O:12])=[CH:7][CH:6]=1>>[Cl:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([N:14]2[CH:19]3[CH2:20][CH2:21][CH2:22][CH:15]2[C:16]2[CH:24]=[N:3][N:2]([CH3:1])[C:17]=2[CH2:18]3)(=[O:13])=[O:12])=[CH:7][CH:6]=1Participants
3
Procedure
Prepared as described in Example 5 using methyl hydrazine and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.
Workup
- customPrepared
- customwas prepared
Sources & evidence
- ORD record
- ord-6c9fc3d5aca747a4acfa7d4a1c2f4d41
- Source dataset
- uspto-grants-2010_07
- Patent number
- US07754712B2
Reaction notes
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