Bis(2-amino-1H-imidazole) sulphate → HCID 66842412, compound

HRID 2354914Notes

Reaction equation

HRID 2354914 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13](=[CH:21]O)[C:14](=O)[CH2:15]3)(=[O:10])=[O:9])=[CH:4][CH:3]=1.S(O)(O)(=O)=O.[NH2:28][C:29]1[NH:30][CH:31]=[CH:32][N:33]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13]2[CH:21]=[N:28][C:29]4[N:33]([C:14]=2[CH2:15]3)[CH:32]=[CH:31][N:30]=4)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 135136Bis(2-amino-1H-imidazole) sulphateHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 66842412HCID 66842412, compound

Procedure

Prepared as described in Example 5 using 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34 and 2-aminoimidazole sulfate.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-d746a195d4ba4b06aa3c0c41714a79a5
Source dataset
uspto-grants-2010_07
Patent number
US07754712B2

Reaction notes

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