HCID 59383129, compound → HCID 86612426, compound

HRID 2355258Notes

Reaction equation

HRID 2355258 reaction equation
[NH:1]1[C:9]2[C:4](=[CH:5][C:6]([O:10][CH2:11][C:12]([O:14][CH3:15])=[O:13])=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.C(OC([N:23]1[C:28]([CH3:30])([CH3:29])[CH2:27][CH2:26]OS1(=O)=O)=O)(C)(C)C>>[NH2:23][C:28]([CH3:30])([CH3:29])[CH2:27][CH2:26][N:1]1[C:9]2[C:4](=[CH:5][C:6]([O:10][CH2:11][C:12]([O:14][CH3:15])=[O:13])=[CH:7][CH:8]=2)[CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 59383129HCID 59383129, compoundHCID 59808925Methyl [(1H-indol-5-yl)oxy]acetate

Product 1

HCID 86612426HCID 86612426, compound

Procedure

Prepared analogously to Component V by alkylation of methyl (1H-indol-5-yloxy)-acetate with N-tert-butoxycarbonyl-4,4-dimethyl-[1,2,3]oxathiazinane-2,2-dioxide and subsequent cleaving of the acid protecting group.

Workup

  1. customPrepared analogously

Sources & evidence

ORD record
ord-f8f4faf5d8ff473992bc875121e3c46d
Source dataset
uspto-grants-2010_07
Patent number
US07754756B2

Reaction notes

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