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HRID 235527作成日：2026年10月25日

Tryptamine hydrochloride → (S)-N-Benzyl-N-methyl-2-[[2-(1H-indol-3-yl)-ethylamino]-N'-(t-butoxycarbonyl)-ethylamino]-3-phenyl-propionamide

https://huagongshe.com/reaction/235527

反応式

関与物質

役割名称HCID仕込み量
反応物Tryptamine hydrochlorideHCID 67652—
反応物HCID 53842533HCID 53842533—
生成物(S)-N-Benzyl-N-methyl-2-[[2-(1H-indol-3-yl)-ethylamino]-N'-(t-butoxycarbonyl)-ethylamino]-3-phenyl-propionamideHCID 86750252—

反応手順

Prepare by the method of Example 1 using 2-(1H-indol-3-yl)-ethylamine hydrochloride salt (tryptamine hydrochloride salt) (0.197 g, 1.0 mmol) and (S)-N-benzyl-N-methyl-2-[N-(t-butoxycarbonyl)-2-oxo-ethylamino]-3-phenyl-propionamide (0.41 g, 1.0 mmol) to give the title compound: TLC Rf =0.69 (silica gel, 85% chloroform/10% methanol/5% acetic acid).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05597845
出典データセットuspto-grants-1997_01
ORD IDord-0003ab746bf54a9f8ba8d633e3decd4c
出典メモuspto-grants-1997_01