HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-Allyloxy-4-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-Allyloxy-4-methoxybenzaldehyde | HCID 534148 | — |
Reaction Steps
The title compound was prepared analogously to 3-ethoxy-4-methyl-benzaldehyde (intermediate E10) by reaction of 3-hydroxy-4-methoxy-benzaldehyde with alkylbromide in DMF using K2CO3 as base (see also A. W. White, R. Almassy, A. H. Calvert, N. J. Curtin, R. J. Griffin, Z. Hostomsky, K. Maegley, D. R. Newell, S. Srinivasan and B. T. Golding J. Med. Chem. 2000, 43, 4084-4097).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754744B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-17976b1e76b34c91851186eaaf652455 |
| Source note | uspto-grants-2010_07 |