HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 22730461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 54705574 | HCID 54705574 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22730461 | HCID 22730461 | — |
Reaction Steps
A solution of Example 296A (2.3 g, 10 mmol) in acetone (300 mL) was treated with iodomethane (5 mL) and K2CO3 (15 g), heated to reflux for 18 hours, and filtered. The filtrate was concentrated and the concentrate purified by flash column chromatography on silica gel with 4:1 hexanes/ethyl acetate to provide the desired product. MS (ESI) m/e 260 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754886B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-e48207648e0649e98aca16850988b1ec |
| Source note | uspto-grants-2010_07 |