HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22730788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Methyl 4'-formyl-2'-methoxy[1,1'-biphenyl]-4-carboxylate | HCID 11558086 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22730788 | HCID 22730788 | — |
Reaction Steps
A solution of Example 122I (270 mg, 0.5 mmol), and sodium borohydride (80 mg) in methanol (5 mL) at room temperature was stirred for 30 minutes, diluted with ethyl acetate (70 mL), washed with water (20 mL) and brine (10 mL), dried (MgSO4), filtered, and concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754886B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-568f0b6a0c514fe6b002012c60e240b8 |
| Source note | uspto-grants-2010_07 |