Triethyl phosphite → HCID 86625203, compound

Participants

Reaction Conditions

Reaction Steps

Under argon, 20 mL of triethyl phosphite was added to 6.1 g (5.8 mmol) of 2-(16-bromohexadecyl)-3,6,7,10,11-pentakishexyloxytriphenylene, and the mixture was stirred at 150° C. for 27 hours. Excess triethyl phosphite was evaporated from the mixture and the residue was purified by silica-gel column chromatography. As a result, 5.4 g of a white solid was obtained.

Provenance & Evidence