HRID2356665

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1(C)NC(=O)N(c2ccc(C#N)c(C(F)(F)F)c2)C1=O

HCID11162285

4-(4,4-Dimethyl-2,5-dioxo-1-imidazolidinyl)-2-(trifluoromethyl)benzonitrile

C13H10F3N3O2

HCID14949936

2-Bromo-1-(bromomethyl)-4-(trifluoromethyl)benzene

C8H5Br2F3

PRODUCTS

生成物

结构：CC1(C)C(=O)N(c2ccc(C#N)c(C(F)(F)F)c2)C(=O)N1Cc1ccc(C(F)(F)F)cc1Br

HCID86633597

未命名化合物

收率 78%

PROCEDURE

实验过程

Compound 55.2 was prepared as described for example 6.2, by reacting compound 1.1 with 2-bromo-4-trifluoromethylbenzyl bromide. 4-[3-(2-Bromo-4-trifluoromethylbenzyl)-4,4-dimethyl-2,5-dioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile was obtained in a yield of 78%. 1H NMR: 8.36, d, 1H, 8.25, s, 1H, 8.1, d, 1H, 8.05, s, 1H; 7.85, d, 1H, 7.73, d, 1H, 4.7, s, 2H, 1.48, s, 6H.