Sodium Hydroxide → HCID 85817901, compound

HRID 2356998Notes

Reaction equation

HRID 2356998 reaction equation
[CH3:1][O:2][C:3](=[O:21])[C:4]1[C:9]([Cl:10])=[CH:8][C:7]([N:11](S(C)(=O)=O)[S:12]([CH3:15])(=[O:14])=[O:13])=[CH:6][C:5]=1[Cl:20].[OH-].[Na+]>C(O)C>[CH3:1][O:2][C:3](=[O:21])[C:4]1[C:9]([Cl:10])=[CH:8][C:7]([NH:11][S:12]([CH3:15])(=[O:14])=[O:13])=[CH:6][C:5]=1[Cl:20]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 85817899HCID 85817899, compound

Product 1

HCID 85817901HCID 85817901, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The mixture of 100 mg of 2,6-dichloro-4-[bis(methanesulfonyl)amino]benzoic acid methylester, 3 ml of an aqueous solution of 1N sodium hydroxide and 10 ml of ethanol was stirred. After the solvent was removed, the obtained substance was treated by an ordinary method using ethyl acetate as an extractant to obtain the title compound.

Workup

  1. customAfter the solvent was removed
  2. additionthe obtained substance was treated by an ordinary method

Sources & evidence

ORD record
ord-ef5d07f061e64192a04d8566e11b5f97
Source dataset
uspto-grants-2010_07
Patent number
US07759388B2

Reaction notes

Loading…