HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → Ethyl (4-acetyl-3-hydroxy-2-propylphenoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 2',4'-Dihydroxy-3'-propylacetophenone | HCID 2775198 | — |
| Product | Ethyl (4-acetyl-3-hydroxy-2-propylphenoxy)acetate | HCID 13389144 | — |
Reaction Steps
1-(2,4-Dihydroxy-3-propyl-phenyl)-ethanone was treated with ethyl 2-bromoacetate and processed as described in the synthesis of example 20a. Yield, 80%, white solid; mp, 61-62° C.; MS (EI): 280 (M+), 265, 251 (100%), 193; analysis: C15H20O5 requires C, 64.27; H, 7.19; found: C, 64.56; H, 7.39%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759387B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-1f5e7f53e8a546228f9bdeda542337b7 |
| Source note | uspto-grants-2010_07 |