1-Tetralone → HCID 390899, compound

HRID 2357151Notes

Reaction equation

HRID 2357151 reaction equation
[C:1]1(=O)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][CH2:2]1.Cl.[CH3:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([NH:21]N)=[CH:17][CH:16]=1>>[CH3:13][O:14][C:15]1[CH:16]=[C:17]2[C:18](=[CH:19][CH:20]=1)[NH:21][C:1]1[C:10]3[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=3[CH2:4][CH2:3][C:2]2=1

Participants

3

Reactant 2

HCID 107241-TetraloneHCID 27239044-Methoxyphenylhydrazine hydrochloride

Product 1

HCID 390899HCID 390899, compound

Procedure

Following the procedure described in Example 4, using 3,4-dihydro-2H-naphthalen-1-one (2.90 g, 20 mmoL) and 4-methoxy-phenylhydrazine HCl salt as the starting material, the title compound was prepared as a brown solid.

Sources & evidence

ORD record
ord-b02302415ef34bec86cdb4efd2651fc4
Source dataset
uspto-grants-2010_07
Patent number
US07759498B2

Reaction notes

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