HCID 59676041, compound → HCID 44412045, compound

HRID 2357191Notes

Reaction equation

HRID 2357191 reaction equation
COC1C=C2C(=CC=1)NC1C3C=CNC=3CCC2=1.C[O:20][C:21]1[CH:22]=[C:23]2[C:31](=[CH:32][CH:33]=1)[N:30]([CH3:34])[C:29]1[C:28]3[CH:35]=[CH:36][N:37]([CH3:38])[C:27]=3[CH2:26][CH2:25][C:24]2=1>>[CH3:38][N:37]1[C:27]2[CH2:26][CH2:25][C:24]3[C:23]4[C:31]([N:30]([CH3:34])[C:29]=3[C:28]=2[CH:35]=[CH:36]1)=[CH:32][CH:33]=[C:21]([OH:20])[CH:22]=4

Participants

3

Reactant 2

HCID 59676041HCID 59676041, compoundHCID 67238823HCID 67238823, compound

Product 1

HCID 44412045HCID 44412045, compound

Procedure

Following the procedure described in Example 125, using 7-methoxy-3,4,5,10-tetrahydro-pyrrolo[3,2-a]carbazole (474 mg, 2.0 mmol) as the starting material, 7-methoxy-3,10-dimethyl-3,4,5,10-tetrahydro-pyrrolo[3,2-a]carbazole as prepared as a crude product. The crude product was thn recated according to the procedure as described in Example 126 to yield the title compound as a brown solid.

Sources & evidence

ORD record
ord-694ea5afd57f4e9cad05fac30c3b48fd
Source dataset
uspto-grants-2010_07
Patent number
US07759498B2

Reaction notes

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