HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 68679077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Reactant | HCID 59639608 | HCID 59639608 | — |
| Product | HCID 68679077 | HCID 68679077 | — |
Reaction Steps
Following the general procedure outlined in Example 193, the product of Example 121 (100 mg, 0.22 mmol), morpholine (58 mg, 0.66 mmol) and trimethylaluminum (0.33 mL, 0.66 mmol) were reacted to give the desired product, 61 mg (64%). LC-MS: 431.2 (MH+, m/z), 2.46 (Rt, min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759486B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-003786a9a0fe410f8bbebc4c631780bb |
| Source note | uspto-grants-2010_07 |