HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → 5-Ethenyl-2-methoxyphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ferulic Acid | HCID 445858 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 5-Ethenyl-2-methoxyphenol | HCID 10441857 | 59% |
Reaction Steps
A mixture of Ferulic acid (0.0083 mol), K2CO3 (10%, 3 ml), imidazole (1 mL) and dimethylformamide (15 ml) were taken in a 250 ml Erlenmeyer flask fitted with a loose funnel at the top. The flask was shaken well and placed inside the microwave oven over an ice bath and irradiated for 30 minutes in parts. After completion of reaction, it was worked up and purified as in example V and provided sweet and pleasant smelling viscous liquid. 59% yield; (Spectral data as in example V)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759527B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-21b7353b9fd14b59afa306d8c6c09164 |
| Source note | uspto-grants-2010_07 |