HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → 5-Sulfoanthranilic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Product | 5-Sulfoanthranilic acid | HCID 19151 | — |
| Product | Disodium | HCID 141233 | — |
Reaction Steps
Anthranilic acid is heated with concentrated sulfuric acid to 180° C. for 1 hour, after which the acid is neutralized with sodium carbonate solution. Evaporation of the water yields the disodium salt of the title compound. Structural verification was obtained by carbon magnetic resonance, proton magnetic resonance and infra-red analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642240 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-95897cff3bc3471fbd44c4e1fb106fac |
| Source note | uspto-grants-1987_02 |